Publications 2017 - 2013

Speciation of very low amounts of antimony in waters using magnetic core-modified silver nanoparticles and electrothermal atomic absorption spectrometry. López-García, S Rengevicova, MJ Muñoz-Sandoval, M. hernández-Cordoba.Talanta 162, 309-315 (2017)

Magnetic solid phase extraction with CoFe2O4/oleic acid nanoparticles coupled to gas chromatography-mass spectrometry for the determination of alkylphenols in baby foods. Marta Pastor-Belda, Pilar Viñas, Natalia Campillo, Manuel Hernández-Córdoba. Food Chemistry 221, 76-81. (2017)

Ten years of dispersive liquid–liquid microextraction and derived techniques. Natalia Campillo, Pilar Viñas, Jana Sandrejov, and Vasil Andruch. Applied Spectroscopy Reviews, VOL. 52, NO. 4, 267–415. (2017)

Glyoxal and methylglyoxal in urine by surfactant-assisted dispersive liquid–liquid microextraction and LC. Natalia Campillo, Pilar Viñas, Javier Marín & Manuel Hernández-Córdoba. Bioanalysis. 9(4), 369-379. (2017)

Combination of solvent extractants for dispersive liquid-liquid microextraction of fungicides from water and fruit samples by liquid chromatography with tandem mass spectrometry. Marta Pastor-Belda, Isabel Garrido, Natalia Campillo, Pilar Viñas, Pilar Hellín, Pilar Flores, José Fenoll. Food Chemistry, 233, 69–76. (2017)

Cloud point microextraction involving graphene oxide for the speciation of very low amounts of chromium in waters. Ignacio López-García, María J. Muñoz-Sandoval, Manuel Hernández-Córdoba.Talanta, 172, 8–14. (2017)

Gas chromatography with mass spectrometry for the determination of phthalates preconcentrated by microextraction based on an ionic liquid. Juan Ignacio Cacho, Natalia Campillo, Pilar Viñas, Manuel Hernández-Córdoba. J. Sep. Sci. 40, 1310–1317. (2017)

Solar detoxification of water polluted with fungicide residues using ZnOcoated magnetic particlesJosé Fenolla, Isabel Garrido, Marta Pastor-Belda, Natalia Campillo, Pilar Viñas, María J. Yañez, Nuria Vela, Simón NavarroChemical Engineering Journal 330, 71–81 (2017)

Triple Quadrupole Mass Spectrometry with Liquid Chromatography and Dispersive
Liquid-Liquid Microextraction for the Determination of Monoterpenes in Alcoholic DrinksAinhoa Oller-Ruiz, Pilar Viñas, Natalia Campillo, José Fenoll & Manuel Hernández-CórdobaFood Analytical Methods 10(10):1-8 (2017)

Glyoxal and methylglyoxal as urinary markers of diabetes. Determination using a dispersive liquid-liquid microextraction procedure combined with gas chromatography-mass spectrometryPastor-Belda M, Fernández-García AJ, Campillo N, Pérez-Cárceles MD, Motas M, Hernández-Córdoba M, Viñas P. J. Chromatogr. A. 1509:43-49 (2017)

Determination of synthetic phosphodiesterase-5 inhibitors by LC-MS2 in waters and human urine submitted to dispersive liquid-liquid microextractionCampillo N, Marín J, Fenoll J, Garrido I, López-García I, Hernández-Córdoba M, Viñas P. Talanta. 174:638-644 (2017)

Dispersive liquid-liquid microextraction for the determination of nitrophenols in soils by microvial insert large volume injection-gas chromatography-mass spectrometry. JI Cacho, N Campillo, P Viñas, M Hernández-Córdoba. Journal of Chromatography A 1456, 27-33 (2016)

Gas chromatography with mass spectrometry for the quantification of ethylene glycol ethers in different household cleaning products. M Pastor‐Belda, N Campillo, M Hernández‐Córdoba, P Viñas. Journal of separation science 39, 2292-2299 (2016)

Use of oleic-acid functionalized nanoparticles for the magnetic solid-phase microextraction of alkylphenols in fruit juices using liquid chromatography-tandem mass spectrometry. P Viñas, M Pastor-Belda, A Torres, N Campillo, M Hernández-Córdoba. Talanta 151, 217-223  (2016)

Control of halophenol and haloanisole concentration in wine cellar environments, wines, corks and wood staves using gas chromatography with mass spectrometry. JI Cacho, J Nicolás, P Viñas, N Campillo, M Hernández‐Córdoba. Australian Journal of Grape and Wine Research 22, 391-398  (2016)

Gas chromatography-mass spectrometry using microvial insert thermal desorption for the determination of BTEX in edible oils. JI Cacho, N Campillo, P Viñas, M Hernández-Córdoba. RSC Advances 6 (25), 20886-20891  (2016)

Determination of synthetic phenolic antioxidants in edible oils using microvial insert large volume injection gas-chromatography. JI Cacho, N Campillo, P Viñas, M Hernández-Córdoba. Food Chemistry 200, 249-254  (2016)

In situ ionic liquid dispersive liquid–liquid microextraction and direct microvial insert thermal desorption for gas chromatographic determination of bisphenol compounds. JI Cacho, N Campillo, P Viñas, M Hernández-Córdoba. Analytical and bioanalytical chemistry 408, 243-249  (2016)

Improved sensitivity gas chromatography–mass spectrometry determination of parabens in waters using ionic liquids. JI Cacho, N Campillo, P Viñas, M Hernández-Córdoba. Talanta 146, 568-574  (2016)

Evaluation of the contamination of spirits by polycyclic aromatic hydrocarbons using ultrasound-assisted emulsification microextraction coupled to gas chromatography-mass spectrometry. JI Cacho, N Campillo, P Viñas, M Hernández-Córdoba. Food Chemistry 190, 324-330  (2016)

Ten years of dispersive liquid–liquid microextraction and derived techniques. N Campillo, P Viñas, J Šandrejová, V Andruch. Applied Spectroscopy Reviews, 1-149  (2016)

A study of the influence on diabetes of free and conjugated bisphenol A concentrations in urine: Development of a simple microextraction procedure using gas chromatography–mass spectrometry. M Pastor-Belda, D Bastida, N Campillo, MD Pérez-Cárceles, M Motas... Journal of Pharmaceutical and Biomedical Analysis 129, 458-465  (2016)

Classification and terminology in dispersive liquid–liquid microextraction. J Šandrejová, N Campillo, P Viñas, V Andruch. Microchemical Journal 127, 184-186  (2016)

Determination of spirocyclic tetronic/tetramic acid derivatives and neonicotinoid insecticides in fruits and vegetables by liquid chromatography and mass spectrometry after dispersive liquid–liquid microextraction. M Pastor-Belda, I Garrido, N Campillo, P Viñas, P Hellín, P Flores... Food chemistry 202, 389-395  (2016)

Direct sample introduction-gas chromatography-mass spectrometry for the determination of haloanisole compounds in cork stoppers. J.I. Cacho, J. Nicolás, P. Viñas, N. Campillo, M. Hernández-Córdoba Journal of Chromatography A 1475, 74-79.  (2016)

Cloud point extraction and gas chromatography with direct microvial insert thermal desorption for the determination of haloanisoles in alcoholic beverages. J.I. Cacho, N. Campillo, P. Viñas, M. Hernández-Córdoba Talanta 160, 282-288.  (2016)

Dispersive liquid–liquid microextraction for the determination of new generation pesticides in soils by liquid chromatography and tandem mass spectrometry, Journal of Chromatography A, 1394, 1–8 (2015)

Determination of phthalate esters in cleaning and personal care products by dispersive liquid–liquid microextraction and liquid chromatography–tandem mass spectrometry, Journal of Chromatography A, 1376, 18–25 (2015)

Cloud point extraction assisted by silver nanoparticles for the determination of traces of cadmium using electrothermal atomic absorption spectrometry, J. Anal. At. Spectrom., 30, 375-380 (2015)


Direct sample introduction gas chromatography and mass spectrometry for the determination of phthalate esters in cleaning products, Journal of Chromatography A, 1380, 156–161 (2015)


Rapid screening of water soluble arsenic species in edible oils using dispersive liquid–liquid microextraction, Food Chemistry, 167, 396–401 (2015)


Determination of Phenolic Acids and Hydrolyzable Tannins in Pomegranate Fruit and Beverages by Liquid Chromatography with Diode Array Detection and Time-of-Flight Mass Spectrometry, Food Anal. Methods, 8, 1315–1325 (2015)

Determination of synthetic phenolic antioxidants in soft drinks by stir-bar sorptive extraction coupled to gas chromatography-mass spectrometry, Food Additives & Contaminants: Part A, 2015, 32, 5, 665–673 (2015)

Determination of very low amounts of free copper and nickel ions in beverages and water samples using cloud point extraction assisted by silver nanoparticles, Anal. Methods, 7, 3786 (2015)


Ultrasound assisted extraction and dispersive liquid–liquid microextraction with liquid chromatography-tandem mass spectrometry for determination of alkylphenol levels in cleaning products, Anal. Methods, 7, 6718 (2015)


Non-chromatographic speciation of chromium at sub-ppb levels using cloud point extraction in the presence of unmodified silver nanoparticles, Talanta, 132, 23–28 (2015)


Dispersive liquid–liquid microextraction for the determination of flavonoid aglycone compounds in honey using liquid chromatography with diode array detection and time-of-flight mass spectrometry, Talanta, 131, 185–191 (2015)

Evaluation of three headspace sorptive extraction coatings for the determination of volatile terpenes in honey using gas chromatography–mass spectrometry, Journal of Chromatography A, 1399, 18–24 (2015)

Recent achievements in solidified floating organic drop microextraction,Trends in Analytical Chemistry, 68, 48–77 (2015)



Speciation of silver nanoparticles and Ag(I) species using cloud point extraction followed by electrothermal atomic absorption spectrometry, Spectrochimica Acta Part B, 101, 93-97 (2014)

A preliminary zonation to support the remediation and the risk assessment of an area contaminated by potentially toxic elements in Murcia Region (SE, Spain), Procedia Earth and Planetary Science, 10, 388-391 (2014)


Dispersive liquid–liquid microextraction in food analysis. A critical review, Analytical Bionalitical Chemistry, 406, 2067-2099 (2014)

Headspace sorptive extraction for the detection of combustion accelerants in fire debris,  Forensic Science International, 238, 26-32 (2014)

Use of headspace sorptive extraction coupled to gas chromatography–mass spectrometry for the analysis of volatile polycyclic aromatic hydrocarbons in herbal infusions, Journal of Chromatography A, 1356, 38-44 (2014)

Capillary liquid chromatography combined with pressurized liquid extraction and dispersive liquid–liquid microextraction for the determination of vitamin E in cosmetic products,  Journal of Pharmaceutical and Biomedical Analysis, 94, 173-179 (2014)

Ultrasound-assisted emulsification microextraction of organolead and organomanganese compounds from seawater, and their determination by GC-MS, Microchim Acta, 181, 97-104 (2014)

Stir bar sorptive extraction polar coatings for the determination of chlorophenols and chloroanisoles in wines using gas chromatography and mass spectrometry, Talanta, 118, 30-36 (2014)

Determination of cadmium and lead in edible oils by electrothermal atomic absorption spectrometry after reverse dispersive liquid–liquid microextraction, Talanta, 124, 106-110 (2014)

Pressurized liquid extraction and dispersive liquid–liquid microextraction for determination of tocopherols and tocotrienols in plant foods by liquid chromatography with fluorescence and atmospheric pressure chemical ionization-mass spectrometry detection, Talanta, 119, 98-104 (2014)

Nonchromatographic Speciation of Selenium in Edible Oils Using Dispersive Liquid−Liquid Microextraction and Electrothermal Atomic Absorption Spectrometry, Journal of Agricultural and Food Chemistry, 61, 9356-9361 (2013)

Stir bar sorptive extraction with gas chromatography–mass spectrometry for the determination of resveratrol, piceatannol and oxyresveratrol isomers in wines Journal of Chromatography, A, 1315, 21-27 (2013)

Dispersive liquid—liquid microextraction for the determination of three cytokinin compounds in fruits and vegetables by liquid chromatography with time-of-flight mass spectrometry Talanta, 116, 376-381 (2013)

Ultrasound-assisted dispersive liquid–liquid microextraction for the speciation of traces of chromium using electrothermal atomic absorption spectrometry Talanta, 115, 166-171 (2013)

Liquid Chromatography with Diode Array Detection and Tandem Mass Spectrometry for the Determination of Neonicotinoid Insecticides in Honey Samples Using Dispersive Liquid−Liquid Microextraction Journal of Agricultural and Food Chemistry, 61, 4799-4805 (2013)

Determination of lead and cadmium using an ionic liquid and dispersive liquid–liquid microextraction followed by electrothermal atomic absorption spectrometry Talanta, 110, 46-52 (2013)

Dispersive liquid-liquid microextraction for the determination of macrocyclic lactones in milk by liquid chromatography with diode array detection and atmospheric pressure chemical ionization ion-trap tandem mass spectrometryJournal of Chromatography A, 1282, 20-26 (2013)

Stir bar sorptive extraction with EG-Silicone coating for bisphenols determination in personal care products by GC–MS Journal of Pharmaceutical and Biomedical Analysis, 78-79, 255-260 (2013)

Dispersive liquid–liquid microextraction for the determination of vitamins D and K in foods by liquid chromatography with diode-array and atmospheric pressure chemical ionization-mass spectrometry detection Talanta, 115, 806-813 (2013)

An evaluation of cis- and trans-retinol contents in juices using dispersive liquid-liquid microextraction coupled to liquid chromatography with fluorimetrie detection Talanta 103, 166-171 (2013)

Headspace sorptive extraction for the analysis of organotin compounds using thermal desorption and gas chromatography with mass spectrometry Journal of Chromatography A, 1279, 1-6  (2013)

Quantification of ß-carotene, retinol, retinyl acetate and retinyl palmitate in enriched fruit juices using dispersive liquid-liquid microextraction coupled to liquid chromatography with fluorescence detection and atmospheric pressure chemical ionization-mass spectrometry, Journal of Chromatography A, 1275,  1-8 (2013)